Articles
THE MAJOR VOLATILE COMPOUNDS OF CRUDE GINGER (ZINGIBER OFFICINALE ROSCOE) EXTRACTS FROM SUPERCRITICAL CO2 EXTRACTION
Article number
875_48
Pages
383 – 386
Language
English
Abstract
This study aims to identify the major volatile compounds of crude ginger extracts from the supercritical carbon dioxide extraction.
Fresh ginger (Zingiber officinale Roscoe) rhizomes were peeled, sliced and dried in a rotary air dryer until containing the moisture content of 9.32±0.23%. Dried gingers were then pulverized to coarse powder approximately 0.5 mm diameter prior to extraction.
The supercritical carbon dioxide extraction of dried ginger was performed at the extraction column with the pressure of 200.0 bar, at the temperature of 35.0°C, followed by series of separation into the 1st and 2nd separating columns with the conditions of 60.0 bar, at 35.0°C and 50.0 bar, at 20.0°C, respectively.
Crude ginger extracts obtained from the 1st and 2nd separating columns were subsequently identified by using gas chromatography-mass spectrometry.
The major volatile compounds of crude ginger extracts were zingiberene (42.97%), AR-curcumene (8.69%), 1,8-cineole (2.58%) and zingerone (4.84% from the 1st separating column, 14.46% from the 2nd separating column).
Fresh ginger (Zingiber officinale Roscoe) rhizomes were peeled, sliced and dried in a rotary air dryer until containing the moisture content of 9.32±0.23%. Dried gingers were then pulverized to coarse powder approximately 0.5 mm diameter prior to extraction.
The supercritical carbon dioxide extraction of dried ginger was performed at the extraction column with the pressure of 200.0 bar, at the temperature of 35.0°C, followed by series of separation into the 1st and 2nd separating columns with the conditions of 60.0 bar, at 35.0°C and 50.0 bar, at 20.0°C, respectively.
Crude ginger extracts obtained from the 1st and 2nd separating columns were subsequently identified by using gas chromatography-mass spectrometry.
The major volatile compounds of crude ginger extracts were zingiberene (42.97%), AR-curcumene (8.69%), 1,8-cineole (2.58%) and zingerone (4.84% from the 1st separating column, 14.46% from the 2nd separating column).
Authors
A. Sirichote, C. Puengphian
Keywords
ginger (Zingiber officinale Roscoe), crude ginger extract, supercritical CO2 extraction
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